Titanium dioxide nanoreactor
HZB
The Henzler team's polymeric nanoreactors consist of a polystyrene core surrounded by a network of PNIPAM chains. A titanium compound was added to an ethanolic solution of the polymer colloids, which did trigger the formation of small titanium dioxide particles within the PNIPAM network. The BESSY II experiments showed that the chemists were able to control the speed of these processes while at the same time affecting the quality of the nanocrystals that had formed.
Using the novel combination of x-ray microscopy and spectroscopy (NEXAFS-TXM, U41-SGM) at BESSY II, Henzler and the microscopy team were able to show that the nanoparticles are homogeneously distributed over the polymeric nanoreactors. The researchers examined their samples in a cryogenic aqueous environment, which prevents artifact formation due to sample drying. Their analysis showed that the nanoparticles have a crystalline structure. "The nanocrystals have a tetragonal anatase structure and this crystalline structure is a key to their catalytic performance.
Additionally, our new analytic method allows us to control the quality of the synthesized particles so that we can optimize them for relevant applications," says Katja Henzler.
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